Development of Differential Pulse Anodic Stripping Voltammetry Technique for Cadmium(II) Detection and Its Application in Water Spinach
نویسندگان
چکیده
Cadmium is a toxic pollutant that harmful to the environment and humans. The purpose of this research was develop method for cadmium(II) detection using differential pulse anodic stripping voltammetry (DPASV) glassy carbon electrode. developed then applied cadmium in vegetable samples which water spinach. optimized several parameters such as potential window, deposition potential, time, scan rate. also investigated its analytical performance includes linearity, precision, limit, quantitation limit. optimum conditions 0.1 M KCl DPASV technique obtained window from -1200 -100 mV, -1100 mV (vs Ag/AgCl), time 360 s. It good linearity with an R2 0.996. precision expressed %SBR 0.66%. limits were 0.4206 µM~0.0771 ppm 0.5525 µM~0.1013 ppm, respectively. measurement spinach sample concentration 0.2399 mg/Kg.
منابع مشابه
Applicability of phenylpiperazine dithiocarbamate in the determination of As(III) in natural water and biological samples by differential pulse anodic stripping voltammetry
An efficient protocol for the selective oxidation of primary alcohols to aldehydes withH5IO6/V2O5 in ionic liquid [bmpy][PF6] has been developed. High yields of the products, mildreaction conditions and simple experimental procedure make this protocol complementary tothe existing methods. The catalyst can be reused for several times without obvious loss of thecatalytic activity.
متن کاملDetermination of Tl(I) Ions in Homeopathic Drugs by Differential Pulse Anodic Stripping Voltammetry
Objectives: The present study is focused on the determination of thallium (I) ions in homeopathic drugs. Methods: The determination was carried out using the Differential Pulse Anodic Stripping Voltammetry (DPASV) technique coupled with the flow-injection measuring system (FIA-DPASV). Results: The thallium content was analyzed in two commercial homeopathic preparations (Thallium aceticum 5CH an...
متن کاملHeavy Metal Analysis by Anodic Stripping Voltammetry
Let’s say that you wanted to determine the heavy metal identities and concentrations in sediment and suspended solid samples obtained from present day Lake Nakuru. What technique would you use for this determination? You could use Atomic Absorption Spectroscopy (AAS) as was done in the article (Nelson 1998), but another technique, which is particularly good at detecting metals at the ppb level ...
متن کاملSimultaneous determination of lead, cadmium, copper and zinc in Infant formula by anodic stripping voltammetry
Determination of trace elements in food is of great importance, as some of them have nutritional significance, whilst others are toxic. Long-term exposure to low levels of toxic metals could be important, especially in relation to children. Differential Pulse Anodic Stripping Voltammetry (DPASV) is applied to simultaneous determination of lead, cadmium, copper and zinc in dry ash infant formula...
متن کاملapplicability of phenylpiperazine dithiocarbamate in the determination of as(iii) in natural water and biological samples by differential pulse anodic stripping voltammetry
an efficient protocol for the selective oxidation of primary alcohols to aldehydes withh5io6/v2o5 in ionic liquid [bmpy][pf6] has been developed. high yields of the products, mildreaction conditions and simple experimental procedure make this protocol complementary tothe existing methods. the catalyst can be reused for several times without obvious loss of thecatalytic activity.
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Indonesian Journal of Chemical Science
سال: 2021
ISSN: ['2614-2627', '2338-5359', '2502-6844']
DOI: https://doi.org/10.30598//ijcr.2020.9-riz